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Meta-talc Application in Inorganic Materials
Bednárek, Jan ; Rovnaník, Pavel (referee) ; Palou, Martin (referee) ; Havlica, Jaromír (advisor)
This thesis is focused at possibilities of preparation and characterization of XRD-amorphous delaminated and dehydroxylated talc phase – meta-talc, which can have its potential application and a starter material for a preparation of magnesium-silicate analogues of geopolymers. Changes in structure and morphology of talc ore were observed during this work. For the purposes of this research, two various talc ores – chloritic and dolomitic were examined. Whole process of meta-talc preparation was examined with whole scale of instrumental techniques such as X-ray diffraction, simultaneous thermogravimetric a differential thermal analysis, infrared spectroscopy, scanning electron microscopy or laser analysis of particle size. Meta-talc can be obtained via mechanochemical activation of talc ore with subsequent calcination. Mechanochemical treatment lead to destruction of original crystal structure and breaking of original bonds, i.e. the product of this treatment was almost amorphous and delaminated. Most of hydroxyl groups were converted to molecules of water which remained adsorbed or coordinated in ore structure. These molecules were removed during calcination step.
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Modern anorganic foundry binder systems
Kolařík, Martin ; Rusín, Karel (referee) ; Cupák, Petr (advisor)
This bachelor thesis deals with newly developed inorganic binder systems. These are mainly developed for their ecological advantages. However, some of the discussed binder systems have better technological properties. Inorganic binder systems are described herein, both on the basis of alkaline silicates and on the basis of inorganic salts. Attention is also paid to bentonite, which is still the most commonly used binder in the world. It turns out that these binder systems will be important for the future of the foundry industry.
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Meta-talc Application in Inorganic Materials
Bednárek, Jan ; Rovnaník, Pavel (referee) ; Palou, Martin (referee) ; Havlica, Jaromír (advisor)
This thesis is focused at possibilities of preparation and characterization of XRD-amorphous delaminated and dehydroxylated talc phase – meta-talc, which can have its potential application and a starter material for a preparation of magnesium-silicate analogues of geopolymers. Changes in structure and morphology of talc ore were observed during this work. For the purposes of this research, two various talc ores – chloritic and dolomitic were examined. Whole process of meta-talc preparation was examined with whole scale of instrumental techniques such as X-ray diffraction, simultaneous thermogravimetric a differential thermal analysis, infrared spectroscopy, scanning electron microscopy or laser analysis of particle size. Meta-talc can be obtained via mechanochemical activation of talc ore with subsequent calcination. Mechanochemical treatment lead to destruction of original crystal structure and breaking of original bonds, i.e. the product of this treatment was almost amorphous and delaminated. Most of hydroxyl groups were converted to molecules of water which remained adsorbed or coordinated in ore structure. These molecules were removed during calcination step.
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|
|
Modern anorganic foundry binder systems
Kolařík, Martin ; Rusín, Karel (referee) ; Cupák, Petr (advisor)
This bachelor thesis deals with newly developed inorganic binder systems. These are mainly developed for their ecological advantages. However, some of the discussed binder systems have better technological properties. Inorganic binder systems are described herein, both on the basis of alkaline silicates and on the basis of inorganic salts. Attention is also paid to bentonite, which is still the most commonly used binder in the world. It turns out that these binder systems will be important for the future of the foundry industry.
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